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Characterization of Mechanically Alloyed Nanocrystalline Fe(Al): Crystallite Size and Dislocation Density

A nanostructured disordered Fe(Al) solid solution was obtained from elemental powders of Fe and Al using a high-energy ball mill. The transformations occurring in the material during milling were studied with the use of X-ray diffraction. In addition lattice microstrain, average crystallite size, dislocation density, and the lattice parameter were determined. Scanning electron microscopy (SEM) was employed to examine the morphology of the samples as a function of milling times. Thermal behaviour of the milled powders was examined by differential scanning calorimetry (DSC). The results, as well as dissimilarity between calorimetric curves of the powders after 2 and 20 h of milling, indicated the formation of a nanostructured Fe(Al) solid solution

Journal of Nanomaterials, 2010, p. 712407

Hindawi Publishing Corporation

Author: Mhadhbi, M.
Khitouni, Mohamed
Escoda i Acero, Ma. Lluïsa
Suñol Martínez, Joan Josep
Dammak, Mohamed Chedly
Date: 2010
Abstract: A nanostructured disordered Fe(Al) solid solution was obtained from elemental powders of Fe and Al using a high-energy ball mill. The transformations occurring in the material during milling were studied with the use of X-ray diffraction. In addition lattice microstrain, average crystallite size, dislocation density, and the lattice parameter were determined. Scanning electron microscopy (SEM) was employed to examine the morphology of the samples as a function of milling times. Thermal behaviour of the milled powders was examined by differential scanning calorimetry (DSC). The results, as well as dissimilarity between calorimetric curves of the powders after 2 and 20 h of milling, indicated the formation of a nanostructured Fe(Al) solid solution
Format: application/pdf
ISSN: 1687-4110 (versió paper)
1687-4129 (versió electrònica)
Document access: http://hdl.handle.net/10256/8573
Language: eng
Publisher: Hindawi Publishing Corporation
Collection: Reproducció digital del document publicat a: http://dx.doi.org/10.1155/2010/712407
Articles publicats (D-F)
Is part of: Journal of Nanomaterials, 2010, p. 712407
Rights: Attribution 3.0 Spain
Rights URI: http://creativecommons.org/licenses/by/3.0/es/
Subject: Nanocristalls -- Propietats tèrmiques
Nanocrystals -- Thermal properties
Title: Characterization of Mechanically Alloyed Nanocrystalline Fe(Al): Crystallite Size and Dislocation Density
Type: info:eu-repo/semantics/article
Repository: DUGiDocs

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